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Moral A, Sicilia MD, Rubio S: Determination of benzimidazolic fungicides in fruits and vegetables by supramolecular solvent-based microextraction/liquid chromatography/fluorescence detection. Anal Chim Acta. 2009 Sep 21;650(2):207-13. Epub 2009 Jul 29.
Carbendazim (CB), thiabendazole (TB) and fuberidazole (FB) were extracted in a single step and no clean-up or concentration of extracts was needed.
They were separated in a Kromasil C18 (5 microm, 150 mm x 4.6 mm) column using isocratic elution [mobile phase: 60:40 (v/v) 50 mM phosphate buffer (pH 4)/methanol] and quantified at 286/320 nm (CB) and 300/350 nm (TB and FB) excitation/emission wavelengths, respectively. |
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