19907098 |
Osaka I, Yoshimoto A, Nozaki K, Moriwaki H, Kawasaki H, Arakawa R: Simultaneous LC/MS analysis of hexachlorobenzene and pentachlorophenol by atmospheric pressure chemical ionization (APCI) and photoionization (APPI) methods. Anal Sci. 2009 Nov;25(11):1373-6. The simultaneous LC/MS analyses of hexachlorobenzene (HCB) and pentachlorophenol (PCP), two dioxin precursors were studied by both atmospheric pressure chemical ionization (APCI) and atmospheric pressure photoionization mass spectrometry (APPI/MS). The optimum LC/MS conditions of the simultaneous analysis were determined for these two compounds with different polarity. Ionization by APPI was found to be more effective than by APCI, and is thus a better ionization method for analysis of the two compounds. Using LC/APPI/MS we can achieve the simultaneous analysis of HCB and PCP at ppb levels. |
14(0,0,2,4) |