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Chen S, Ocampo AP, Kucera PJ: Liquid chromatographic method for the determination of calcium cyanamide using pre-column derivatization. J Chromatogr. 1991 Sep 27;558(1):141-6. A specific and stability-indicating high-performance liquid chromatographic (HPLC) method has been developed for the analysis of calcium cyanamide in bulk material and dosage form. Calcium cyanamide in samples was converted into dansyl cyanamide. A muBondapak C18 column was employed for HPLC with 0.01 M sodium phosphate (pH 6.3)-acetonitrile (75:25, v/v) as the mobile phase. The proposed HPLC method was validated for linearity, specificity, accuracy and reproducibility. |
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